Last edited by Met
Wednesday, May 13, 2020 | History

2 edition of Calibration of Volumetric Glassware found in the catalog.

Calibration of Volumetric Glassware

Atomic Energy of Canada Limited.

Calibration of Volumetric Glassware

A Discussion and Procedure.

by Atomic Energy of Canada Limited.

  • 254 Want to read
  • 17 Currently reading

Published by s.n in S.l .
Written in English


Edition Notes

1

SeriesAtomic Energy of Canada Limited. AECL -- 7991
ContributionsKramer, G., Robinson, P.
ID Numbers
Open LibraryOL21969317M

This practice covers procedures for use in the calibration of volumetric ware, in accordance with Specification E such as is in common use in chemical and clinical laboratories. It is based on the gravimetric determination of the quantity of water either contained or delivered, and the conversion of this value to true volume at the standard temperature of 20°C by means of suitable. Calibration of Measuring Flasks or Small Provers using Volume Transfer Methods SOP 18 Calibration of Graduated Neck-Type Metal Volumetric Field Standards, Volumetric Transfer Method SOP 19 Calibration of Large Neck-Type Metal Provers, Volume Transfer Method SOP 20 Control Charts for Calibration of Neck Type Provers, Volume.

For greatest accuracy, volumetric glassware should be calibrated to measure the volume that is actually contained in or delivered by a particular piece of glassware. The calibration is done by measuring the mass of water contained in or delivered by the glassware. The density of water at a particular temperature is used to convert mass into volume.   Basic principles of Glassware Calibration• Calibration up to manufacturer – Capacity marks/graduation • Lines marked on volume measuring devices that indicate volume – Lines the way to make the measurements – Determined by American Society for Testing and Materials (ATSM) • Meniscus – Must be considered – A curve formed by the.

  This video outlines how to calibrate and use a volumetric pipet. For more information on our program, visit Although glass is virtually resistant to all other common chemicals, e.g. organic solvents, water and acids, glass will be slightly degraded with a very small depth of erosion over a relatively long time (Figure 1). Subject to this effect, glass volumetric instruments have to be monitored regularly in order to get reliable results. Figure 1.


Share this book
You might also like
Hollywood Legs

Hollywood Legs

Core financial system requirements

Core financial system requirements

German Aircraft World War 2

German Aircraft World War 2

Bad Dreams/good Girl

Bad Dreams/good Girl

origin of terrestrial vertebrates

origin of terrestrial vertebrates

Using tapes at NIH

Using tapes at NIH

Long courses for teachers.

Long courses for teachers.

Principles of color photography [by] Ralph M. Evans, W.T. Hanson, Jr. [and] W. Lyle Brewer.

Principles of color photography [by] Ralph M. Evans, W.T. Hanson, Jr. [and] W. Lyle Brewer.

Be authentic

Be authentic

Elizabethan stage.

Elizabethan stage.

Letter from the Secretary of War inclosing three statements of the amount of merchandise and supplies purchased on behalf of the United States

Letter from the Secretary of War inclosing three statements of the amount of merchandise and supplies purchased on behalf of the United States

Air (The Four Elements)

Air (The Four Elements)

Calibration of Volumetric Glassware by Atomic Energy of Canada Limited. Download PDF EPUB FB2

Calibrating Volumetric Glassware ** Volumetric glassware is calibrated by measuring the mass of a liquid (usually distilled or de Calibrating Volumetric Glassware ** Volumetric glassware is calibrated by measuring the mass of a liquid (usually distilled or deionized water) of known density and temperature that is contained in (or delivered by) the volumetric ware.

Calibration of Volumetric Glassware This set of laboratory experiments is designed to introduce you to some of the apparatus and operations you will be using during the remainder of this course, including the treatment ofFile Size: KB.

All volumetric glassware for quantitative work requires calibration. Range All volumetric glassware used for accurate delivery or to contain specific volumes needs to be calibrated. Apparatus and Equipment Analytical balance accurate to mg (g) Analytical balance accurate to g. (For volumes of mL or less, the balance File Size: KB.

By convention, volumetric glassware is always calibrated at 20 °C. Since the temperature at which you do the calibration may be somewhat different there is Calibration of Volumetric Glassware book small correction for the cubic coefficient of expansion of glass.

Fortunately the correction isFile Size: KB. If the volumetric glassware is not within the limits of calibration discard the glassware. Precautions: Use clean and dried volumetric glassware at the time of calibration.

Ensure that the glassware is maintained at 27° C at the time of calibration. Use lower meniscus for : Nabl Guideline. Calibration of volumetric flasks Weigh a clean & dry volumetric flask. Calibrate the flask by filling it with recently boiled and cooled distilled water at room temperature up to the mark and weigh the flask.

Determine the volume in ml by the formula. All Pyrex ® and MBL ® volumetric glassware is calibrated at 20°C. If the product is calibrated to Class A/AS accuracy tolerances, it is usually marked with a batch or individual serial number for identification and traceability.

Pyrex ® and MBL ® volumetric flasks are also marked with the date of. Calibration of volumetric flasks. Weigh empty, dry flask. Fill it with distilled water to mark.

Weigh again. Mass difference is the mass of water. Repeat times. Calibration of single volume pipettes. Weigh empty, dry, closed weighing bottle.

Pipette water into the bottle, close, weigh again. Mass difference is the mass of water. Repeat times. Calibration of Volumetric Glassware Introduction The purpose of Calibrating Volumetric Glassware lab was to learn how to use volumetric glassware properly for future labs.

Knowing how to use equipment is always a good aspect in lab because it helps cause better use, precision, accuracy, and time efficiency. It is very important to calibrate measuring apparatuses prior to use because every.

Based on the result, the average volume of calibration of 10 mL volumetric pipette is mL. The average volume of calibration of 25 mL volumetric pipette is mL. Then, the average volume of calibration of mL of volumetric flask is mL.

So, the average volume of 50 mL measuring cylinder is mL. This experiment aimed at calibrating volumetric glassware (Mohr pipette) by comparing its volume capacity with the calculated volume of liquid delivered. Theoretical volume was determined by dividing the mass of liquid by its reference density at a.

Calibration of Glassware Calibration of volumetric apparatus at specified intervals is an important task. Volume, weight and delivery time at calibration temperature are.

Volumetric Flask; Transfer pipettes Burettes; Before using Class ‘B’ apparatus, they should be calibrated as following all step during calibration of glassware the water temperature should be 25 °C.

Calibration procedure: Take all volumetric flasks up to mL, transfer pipettes, Burettes for calibration. For volumetric flask. Objective To ensure that the glassware used for analysis is accurate and is within the tolerance limits of nominal volume.

Scope This procedure is applicable for all glassware (Burette, pipette & volumetric flask) to be used in quality control laboratory. Lab Report: Calibration of Volumetric Glassware Essay Words 7 Pages Calibration of Volumetric Glassware Nur Farah Nabilah Binti Ahmed Zhaini Muhammad Imanuddin Bin Azman Maisarah Binti Alias Summary In this experiment, The purpose of this experiment is to investigate the measurement of the actual volume contents of volumetric glassware.

CHEM LQuantitative Analysis LaboratoryRevision Calibration of Volumetric GlasswareIn this laboratory exercise, we will calibrate the three types of glassware typically used by ananalytical chemist; a volumetric flask, a volumetric pipet and a buret.

Calibration of Volumetric Glassware Read: Chapters in Harris to be prepared for the laboratory experiment. This experiment is designed to introduce you to proper analytical laboratory techniques and to the methods for evaluating analytical data.

As an analytical chemist, it isFile Size: KB. for volumetric instruments to be uti-lized. A most important requirement of the USP is the mandatory use of glass volumetric instruments with accuracy according to class A.

Due to some clauses this seemingly easy demand eventually turns out to be difficult to understand. On the one hand, the require-ments for volumetric flasks, transfer. Subject:Analytical Chemistry/Instrumentation Paper: Fundamentals of Analytical Chemistry. Calibration procedure for Volumetric Flasks Calibration Should be carried out at 25±2 ⁰C.

Tare the weigh balance. Weigh the empty volumetric flask and record value in gm. And note if this is Class-A or other grade.

Fill the volumetric flask up to mark with distilled water, and re-weigh it. Measure the temperature of the water used. Repeat. In all step during calibration of glassware the water temperature should be 25 °C.

Calibration procedure: Take all volumetric flasks up to mL, transfer pipettes, Burettes for calibration. For volumetric flask: Weigh accurately a previously dried volumetric flask.Calibration of Glassware Introduction Glassware is commonly calibrated using a liquid of known, specific density, and an analytical balance.

The procedure is to determine the mass of liquid the glassware will hold, and to divide this mass of liquid by the density of the liquid, obtaining the corresponding volume of liquid. Density.Table 2b Data for Calibration of a 50 mL Buret.

Temperature of Water: Mass of Flask + Stopper (g): Initial Volume (mL): Mass of Flask, Stopper, Sample (g) Mass of Sample (g) Final Volume (mL) Total Volume Dispensed (mL) 2. Fill a buret with distilled water that has been equilibrated to room temperature and force any air bubbles out the Size: 86KB.